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상용순수 타이타늄과 Ti-6Al-4V 합금의 마찰접합 특성에 관한 연구

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Author(s)
김경우
Issued Date
2022
Keyword
friction welding, titanium and its alloy, electron backscattered diffraction method, mechanical properties, microstructures
Abstract
In this study, a systematic investigation on the microstructural evolution and mechanical properties in the weld zone of similar and dissimilar joint of commercial pure (CP) titanium and Ti-6Al-4V alloy welded by friction welding (FW) was carried out.
Specimens with a diameter of 15 mm and length of 50 mm were prepared, FW was performed at constant rotation speed changing different process parameters such as friction pressure, upset pressure, and upset length. The electron backscattered diffraction (EBSD) method was used to analyze the grain boundary characteristic distributions (GBCDs) such as grain size, misorientation angle, orientation, and phase distributions. Mechanical properties of each joint were evaluated using the microhardness and tensile tester.
It was found that the application of the similar FW to CP titanium led to significantly refined grains, of which the average size is 0.71 μm, in the weld zone while that of the base material was 11.4 μm. The grain orientation was changed from <0001> in base material to <21 ̅1 ̅0> in the weld zone. These microstructural evolutions resulted from the dynamic recrystallization caused by frictional heat and material flow during FW. On the contrary, microstructures in the weld zone of Ti-6Al-4V alloy during similar FW were developed by combination effect of dynamic recrystallization and phase transformation. Consequently, the microstructures in the weld zone consisted of equiaxed and lamellar structures, and its grains (1.4 μm) were markedly refined compared to that of base material (5.74 μm).
Dissimilar FW between CP titanium and Ti-6Al-4V alloy was carried out. It was found that the microstructures in the weld zone at the CP titanium and Ti-6Al-4V alloy were differently developed due to the different thermal conductivity of each material. Microstructures in the weld zone at CP titanium side were changed in the same way as those during the similar FW while those at Ti-6Al-4V alloy side were differently developed due to the fragmentation resulted from insufficient heat-input. The average grain sizes in the weld zone at both sides of CP titanium and Ti-6Al-4V alloy were 1.03 μm and 1.01 μm, respectively. Because of the refined grains, the micro-hardness in the weld zone of similar and dissimilar titanium joints were higher than those of initial materials. Besides, the yield and tensile strengths were maintained at the same levels as those of the base materials. The tensile specimens were fractured at base materials not at the weld zone or heat-affected zone.
The microstructures and mechanical properties of welds for similar and dissimilar joint using FW were investigated. Through this study, it was found that the continuous dynamic recrystallization, which determined the characterization of the final microstructure in weld zone, was dominant recrystallization phenomenon during FW. The strengthening mechanism by applying FW is expected to give insight into securing the titanium joints with superior performance. Furthermore, the results of the microstructures and mechanical properties obtained through this study are expected to be used for basic research data for the reliability evaluation of dissimilar titanium joint and for the study on dissimilar solid-state welding between α and α+βphase titanium alloys.
Alternative Title
Study on properties of friction welding of commercially pure titanium and Ti-6Al-4V alloy
Alternative Author(s)
Gyeong-Woo Kim
Affiliation
조선대학교 일반대학원
Department
일반대학원 선박해양공학과
Advisor
정세민
Awarded Date
2022-08
Table Of Contents
List of figures IV
List of tables X
ABSTRACT XI

제 1장 서론 1
1.1 연구배경 및 필요성 1
1.2 이론적 배경 및 문헌조사 6
1.2.1 타이타늄과 타이타늄 합금 6
1.2.2 고상접합기술 17
1.2.3 타이타늄과 타이타늄 합금의 마찰접합 연구동향 24
1.2.4 동적재결정(dynamic recrystallization)메커니즘 29
1.3 연구목적 및 내용 35
1.4 본 연구의 구성 36

제 2장 실험방법 38
2.1 연구에 사용된 재료 38
2.2 마찰접합장비와 공정조건 설계 40
2.3 미세조직분석 43
2.3.1 광학현미경 43
2.3.2 EBSD분석 43
2.4 마찰접합재의 기계적 특성 평가 45
2.4.1 미세 경도시험 45
2.4.2 인장시험 45

제 3장 마찰접합된 상용 타이타늄의 미세조직과 기계적 특성 평가 48
3.1 서언 48
3.2 결과 및 고찰 49
3.2.1 초기재료분석 49
3.2.2 CP-Ti-2 마찰접합재의 외관 검사 51
3.2.3 광학현미경을 이용한 상용 타이타늄 마찰접합재의 단면 분석 56
3.2.4 접합부 미세조직 특성 61
3.2.5 마찰접합재의 기계적 특성 평가 73
3.3 요약 79

제 4장 마찰접합된 Ti-6Al-4V 합금의 미세조직과 기계적 특성 80
4.1 서언 80
4.2 결과 및 고찰 81
4.2.1 초기재료 분석 81
4.2.2 Ti-6Al-4V 합금 마찰접합재의 외관 검사 83
4.2.3 광학현미경을 이용한 Ti-6Al-4V 합금 마찰접합재 단면 분석 86
4.2.4 접합부 미세조직 특성과 미세조직의 발달 양상 89
4.2.5 마찰접합재의 기계적 특성 105
4.3 요약 112

제 5장 이종 타이타늄 마찰접합재의 미세조직과 기계적특성 평가 113
5.1 서언 113
5.2 결과 및 고찰 114
5.2.1 광학현미경을 이용한 이종 마찰접합재 단면 분석 114
5.2.2 이종 마찰접합재의 접합부 미세조직 특성 116
5.2.3 이종 마찰접합재의 기계적특성 132
5.2.4 접합부 미세조직의 발달 양상 136
5.2.5 이종마찰접합재의 기계적물성 강화 142
5.3 요약 147

제 6장 결론 148

Reference 150
Degree
Doctor
Publisher
조선대학교 대학원
Citation
김경우. (2022). 상용순수 타이타늄과 Ti-6Al-4V 합금의 마찰접합 특성에 관한 연구.
Type
Dissertation
URI
https://oak.chosun.ac.kr/handle/2020.oak/17431
http://chosun.dcollection.net/common/orgView/200000638298
Appears in Collections:
General Graduate School > 4. Theses(Ph.D)
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